Polymer Sequence Determination : Carbon-13 NMR Method
Polymer Sequence Determination : Carbon-13 NMR Method
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Author(s): Randall, James
Randall, James C.
ISBN No.: 9780125780506
Pages: xiii, 155
Year: 197802
Format: Trade Cloth (Hard Cover)
Price: $ 36.15
Status: Out Of Print

PrefaceAcknowledgments1 Polymer Structure and Carbon-13 NMR 1.1 Configurational Sequences in Vinyl Homopolymers 1.2 Carbon-13 Chemical Shift Behavior in Vinyl Homopolymers 1.3 Configurational Sequence Lengths and Carbon-13 Line Multiplicity 1.4 Configurational Assignments in Polypropylene2 Number-Average Sequence Lengths in Vinyl Polymers 2.1 Number-Average Sequence Lengths of Like Configurations 2.2 Number-Average Sequence Lengths of Meso and Racemic Additions 2.3 NMR Measurements of ?umber-Average Sequence Lengths3 Number-Average Sequence Lengths in Copolymers and Terpolymers 3.


1 ?umber-Average Sequence Lengths in Copolymers and Dyad Concentrations 3.2 Copolymer Number-Average Sequence Lengths and Triad Concentrations 3.3 Number-Average Sequence Lengths in Hydrogenated Polybutadienes 3.4 Monomer Distributions and Number-Average Sequence Lengths in Ethylene-Propylene Copolymers 3.5 Number-Average Sequence Lengths and Dyad Distributions in Terpolymers 3.6 ?umber-Average Sequence Lengths and Triad Distributions in Terpolymers 3.7 ?umber-Average Sequence Lengths in Hydrogenated Butadiene-Styrene Copolymers4 Statistical Analyses of Monomer Distributions and Number-Average Sequence Lengths 4.1 Bernoullian Statistical Analyses 4.


2 First-Order Markov Statistical Analyses of Copolymers 4.3 Statistical Analyses of Hydrogenated Polybutadienes 4.4 Statistical Analyses of Configurational Sequences in Vinyl Homopolymers 4.5 A Statistical Analysis of Configurational Sequences in Atactic Polystyrenes5 Experimental Design for Quantitative FT-NMR Measurements 5.1 Saturation and Resolution in FT-NMR 5.2 The Nuclear Overhauser Effect and Carbon-13 Natural Abundance 5.3 Intensity Measurements in FT-NMR Quantitative Studies 5.4 Computer Requirements in FT Quantitative Studies6 A Survey of Carbon-13 NMR Studies of Vinyl Homopolymers and Copolymers 6.


1 Poly(Vinyl Chloride) 6.2 Poly(Vinyl Alcohol) 6.3 Poly(Vinyl Acetate) 6.4 Poly(Methyl Methacrylate) 6.5 Poly(a-Methylstyrene) 6.6 Polystyrene 6.7 Poly(Methyl Acrylate) 6.8 Poly(Isopropyl Acrylate) 6.


9 Poly(Methyl Vinyl Ether) 6.10 Poly(Ethyl Vinyl Ether) 6.11 Poly(Isopropyl Vinyl Ether) and Poly(Isobutyl Vinyl Ether) 6.12 Poly(Tert-Butyl Vinyl Ether) 6.13 Poly(Methacrylonitrile) 6.14 Polyacrylonitrile 6.15 Trends among Configurational Assignments in Vinyl Homopolymers 6.16 Ethylene-Propylene Copolymers 6.


17 Ethylene-Vinyl Acetate Copolymers 6.18 Acrylonitrile-Styrene Copolymers 6.19 Butadiene-Styrene CopolymersReferencesIndex.


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