Polymer Sequence Determination: Carbon-13 NMR Method covers the principles, practice, and application of 13C NMR to polymer structure determination. This book is divided into six chapters that highlight spectral interpretations, applications, and experimental considerations.Chapter 1 examines the polymer structure, with special emphasis on those structural features delineated by 13C NMR, along with the assignment techniques used during 13C NMR interpretationsof polymer spectra. Chapters 2 and 3 present the methods for measuring sequence distributions and number-average sequence lengths for configurational sequences in vinyl homopolymers and for the comonomer distribution in copolymers and terpolymers. Chapter 4 discusses the statistical approaches to polymer characterization, while Chapter 5 contains practical experimental considerations when designing an NMR experiment to obtain quantitative structural information. Chapter 6 reviews 13C NMR studies for various vinyl homopolymers and copolymers. This book will be of great value to polymer scientists, NMR spectroscopists, and researchers.